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CEN/TS 15968:2010

Determination of extractable perfluorooctanesulphonate (PFOS) in coated and impregnated solid articles, liquids and fire fighting foams - Method for sampling, extraction and analysis by LC-qMS or LC-tandem/MS

Edition date: 2023-11-22
Cancelled
Available languages: German, English
Summary: La présente Spécification technique européenne décrit la détermination du sulfonate de perfluorooctane (SPFO) dans un extrait concentré provenant d’articles solides couchés et imprégnés, de liquides et de mousses anti-incendie au moyen d’une chromatographie en phase liquide haute performance couplée à la spectrométrie de masse en tandem (LC-MS/MS) ou à une spectrométrie de masse quadripôle (LC-MS). La méthode est applicable pour une plage de concentration de SPFO dans la solution d’extrait allant de 0,5 ng/ml à 50 ng/ml. AVERTISSEMENT — Il convient que les utilisateurs de la présente Spécification technique soient familiarisés avec les pratiques courantes de laboratoire. La présente Spécification technique n’a pas pour objet de traiter tous les problèmes de sécurité qui sont, le cas échéant, liés à son utilisation. Il incombe à l’utilisateur d’établir des pratiques appropriées en matière d’hygiène et de sécurité et de s'assurer de la conformité à la réglementation nationale en vigueur. IMPORTANT — Il est absolument essentiel que les essais menés conformément à la présente Spécification technique soient effectués par un personnel qualifié.

This Technical Specification describes the determination of perfluorooctanesulfonate (PFOS) in concentrated extracts from coated and impregnated solid articles, liquids and fire extinguishing foams using high performance liquid chromatography-tandem mass spectrometry (LC-tandemMS) or quadrupole mass spectrometry (LC-qMS). The method is applicable for a concentration range for PFOS in the extract solution of 0,5 µg/l to 50 µg/l. WARNING - Persons using this Technical Specification should be familiar with normal laboratory practice. This Technical Specification does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions. IMPORTANT - It is absolutely essential that tests conducted in accordance with this Technical Specification be carried out by suitably qualified staff.

Die vorliegende Technische Spezifikation beschreibt die Bestimmung von Perfluoroctansulfo¬nat (PFOS) in konzentrierten Extrakten aus beschichteten und imprägnierten Feststoffartikeln, Flüssigkeiten und Feuerlöschschäumen unter Anwendung von Hochleistungs-Flüssigkeitschromatographie/Tandem-Massen-spektrometrie (LC tandem/MS) oder Quadrupol-Massenspektrometrie (LC qMS). Das Verfahren ist anwendbar auf Konzentrationen von PFOS in der Extraktionslösung im Bereich zwischen 0,5 µg/l und 50 µg/l. WARNUNG - Die Anwender dieser Technischen Spezifikation sollten mit der üblichen Laborpraxis vertraut sein. Diese Technische Spezifikation beansprucht nicht, sämtliche mit deren Anwendung verbundenen Sicherheitsprobleme, soweit solche gegeben sind, abzudecken. Es liegt in der Verantwortung des Anwenders, geeignete Maßnahmen für Gesundheits- und Arbeitsschutz einzuleiten und deren Übereinstimmung mit sämtlichen nationalen gesetzlichen Vorschriften sicherzustellen. WICHTIG - Es ist unbedingt notwendig, dass Prüfungen nach dieser Technischen Spezifikation von entspre¬chend qualifizierten Personen durchgeführt werden.
ICS: 71.080.20-Halogenated hydrocarbons, 71.040.50-Physicochemical methods of analysis
CTN: CEN/TC 248 - 6229

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