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CEN/TS 15606:2009

Foodstuffs - Determination of acesulfame-K, aspartame, neohesperidine-dihydrochalcone and saccharin - High performance liquid chromatographic method

Edition date: 2012-05-04
In Force
Available languages: English, French, German
Summary: Diese Technische Spezifikation (prCEN/TS 15606:2009) legt ein hochleistungs-flüssigchromatographisches (en: high performance liquid chromatographic, (HPLC)) Verfahren zur Bestimmung von Acesulfam-K, Aspartam, Neohesperidin-Dihydrochalcon und Saccharin in Lebensmitteln fest. Das Verfahren ist für das Dialyseverfahren vollständig in einem Ringversuch nach dem IUPAC Harmonized Protocol [2] für die folgenden Analyt/Matrix-Kombinationen validiert worden [1]: - Acesulfam-K und Aspartam in Getränken auf Wasserbasis, Fruchtsaftgetränken, Käsekuchen mit Biskuit-boden, Dosensuppen und Schokoladengetränkepulver; - Saccharin in Getränken auf Wasserbasis, Fruchtsaftgetränken, Käsekuchen mit Biskuitboden und Dosen-suppen; - Neohesperidin-Dihydrochalcon in Getränken auf Wasserbasis, Fruchtsaftgetränken und Dosensuppen.

This Technical Specification (prCEN/TS 15606:2009) specifies a high performance liquid chromatographic (HPLC) method for the determination of acesulfame-K, aspartame, neohesperidine-dihydrochalcone and saccharin in foodstuffs. The method has been fully validated [1] for the dialysis procedure through collaborative trial, according to the IUPAC Harmonised Protocol [2], on the following analyte matrix combinations: acesulfame-K and aspartame in water-based drink, fruit-based drink, cheesecake with biscuit base, canned soup and instant chocolate drink; saccharin in water-based drink, fruit-based drink, cheesecake with biscuit base and canned soup; neohesperidine-dihydrochalcone in water-based drink, fruit-based drink and canned soup.

liquide haute performance (CLHP) avec détection UV pour le dosage de l'acésulfame-K, de l'aspartame, de la néohespéridine dihydrochalcone et de la saccharine dans les produits alimentaires. La méthode a été entièrement validée [1] pour la technique de dialyse au moyen d'un essai interlaboratoire (voir 8.2, 8.3 et Annexe C) réalisé, conformément au Protocole Harmonisé [2] de l'UICPA, sur les combinaisons analytematrice suivantes : - acésulfame-K (de 86 mg/l à 331 mg/l) et aspartame (de 97 mg/kg à 610 mg/l) dans une boisson à base d'eau, une boisson à base de fruits, un gâteau au fromage blanc à base de biscuit, un potage en boîte et une boisson chocolatée instantanée ; - saccharine (de 70 mg/l à 97 mg/kg) dans une boisson à base d'eau, une boisson à base de fruits, un gâteau au fromage blanc à base de biscuit et un potage en boîte ; - néohespéridine dihydrochalcone (de 27 mg/l à 57 mg/kg) dans une boisson à base d'eau, une boisson à base de fruits et un potage en boîte.
ICS: 67.050-General methods of tests and analysis for food products
CTN: CEN/TC 275 - 6256

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