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ASTM D1238 - 13
Standard Test Method for Melt Flow Rates of Thermoplastics by Extrusion Plastometer
| Aviso: | Las normas ASTM en lectura se visualizan a través del área decliente. Los archivos no se pueden descargar |
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| Fecha edición: |
2013-08-01
Anulada
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| Fecha cancelación: | 2013-08-01 |
| Idiomas disponibles: | Inglés |
| Resumen: | |
| Keywords: | melt flow rate; melt index; volume flow rate |
| Scope: | 1.1 This test method covers the determination of the rate of extrusion of molten thermoplastic resins using an extrusion plastometer. After a specified preheating time, resin is extruded through a die with a specified length and orifice diameter under prescribed conditions of temperature, load, and piston position in the barrel. Four procedures are described. Comparable results have been obtained by these procedures in interlaboratory round-robin measurements of several materials and are described in Section 15. 1.2 Procedure A is used to determine the melt flow rate (MFR) of a thermoplastic material. The units of measure are grams of material/10 minutes (g/10 min). It is based on the measurement of the mass of material that extrudes from the die over a given period of time. It is generally used for materials having melt flow rates that fall between 0.15 and 50 g/10 min (see Note 1). 1.3 Procedure B is an automatically timed measurement used to determine the melt flow rate (MFR) as well as the melt volume rate (MVR) of thermoplastic materials. MFR measurements made with Procedure B are reported in g/10 minutes. MVR measurements are reported in cubic centimetres/ten minutes (cm3/10 min). Procedure B measurements are based on the determination of the volume of material extruded from the die over a given period of time. The volume is converted to a mass measurement by multiplying the result by the melt density value for the material (see Note 2). Procedure B is generally used with materials having melt flow rates from 0.50 to 1500 g/10 min. 1.4 Procedure C is an automatically timed measurement used to determine the melt flow rate (MFR) of polyolefin materials. It is generally used as an alternative to Procedure B on samples having melt flow rates greater than 75 g/10 min. Procedure C involves the use of a modified die, commonly referred to as a “half-die,” which has half the height and half the internal diameter of the standard die specified for use in Procedures A and B thus maintaining the same length to diameter ratio. The test procedure is similar to Procedure B, but the results obtained with Procedure C shall not be assumed to be half of those results produced with Procedure B. 1.5 Procedure D is a multi-weight test commonly referred to as a “Flow Rate Ratio” (FRR) test. Procedure D is designed to allow MFR determinations to be made using two or three different test loads (either increasing or decreasing the load during the test) on one charge of material. The FRR is a dimensionless number derived by dividing the MFR at the higher test load by the MFR at the lower test load. Results generated from multi-weight tests shall not be directly compared with results derived from Procedure A or Procedure B. Note 1—Polymers having melt flow rates less than 0.15 or greater than 900 g/10 min may be tested by the procedures in this test method; however, precision data have not been developed. Note 2—Melt density is the density of the material in it molten state. It is not to be confused with the standard density value of the material. See Table 3. |
| ICS: | 83.080.20 - Materiales termoplásticos |
| CTN: | D20.30 - D20.30 |
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Otras Relaciones |
Es referenciada por D3275-18R23 Es referenciada por D5138-23 Es referenciada por D3485-22 Es referenciada por D6265-23 Es referenciada por D3035-22 Es referenciada por F3123-22 Es referenciada por D7238-20 Es referenciada por F2881_F2881M-21E01 Es referenciada por D6394-21A Es referenciada por F0561-19 Es referenciada por D3159-22 Es referenciada por D5577-19 Es referenciada por F0755-19 Es referenciada por D2116-16R21 Es referenciada por D7082-21 Es referenciada por D6388-18 Es referenciada por F2619_F2619M-20 Es referenciada por D5990-20A Es referenciada por D3935-21 Es referenciada por D4565-20 |









